Fabrication and application of surface enhanced Raman scattering substrates by oblique angle deposition
ZHANG Zheng-jun1, XIE Zheng1,2
(1. Key Laboratory of Advanced Materials MOE, School of Materials Science and Engineering, Tsinghua University, Beijing 100084,China 2.High-Tech Institute of Xi’an, Xi’an 710025, Shaanxi,China)
Abstract:Noble metals nanostructures are wildly used in detection of trace chemicals based on the surface enhanced Raman scattering. The controllable fabrication of Ag nanorod arrays by oblique angle deposition and their application in detection of trace chemicals were introduced, and the semi-quantitative and quantitative analysis of trace chemicals were established by principal component analysis and partial least squared regression methods.
[1] KRISHNAN K S. A New Type of Secondary Radiation [J]. Nature, 1928, 121(3048): 501-2.[2] FLEISCHMANN M, HENDRA P J, MCQUILLAN A J. Raman spectra of pyridine adsorbed at a silver electrode [J]. Chemical Physics Letters, 1974, 26(2): 163-6.[3] JEANMAIRE D L, DUYNE R P V. Surface raman spectroelectrochemistry : Part I. Heterocyclic, aromatic, and aliphatic amines adsorbed on the anodized silver electrode [J]. Journal of Electroanalytical Chemistry & Interfacial Electrochemistry, 1977, 84(1): 1-20.[4] ALBRECHT M G, CREIGHTON J A. ChemInform Abstract: ANOMALOUSLY INTENSE RAMAN SPECTRA OF PYRIDINE AT A SILVER ELECTRODE [J]. Journal of the American Chemical Society, 1977, 8(44): no-no.[5] KLEINMAN S L, FRONTIERA R R, HENRY A I, et al. Creating, characterizing, and controlling chemistry with SERS hot spots [J]. Physical Chemistry Chemical Physics, 2013, 15(1): 21-36.[6] MOSKOVITS M. Surface‐enhanced Raman spectroscopy: a brief retrospective [J]. Journal of Raman Spectroscopy, 2005, 36(6-7): 485-96.[7] LE RU E C, ETCHEGOIN P G. Chapter 1 - A quick overview of surface-enhanced Raman spectroscopy [M]. Principles of Surface-Enhanced Raman Spectroscopy. Amsterdam; Elsevier. 2009: 1-27.[8] MICHEL O, TAEKJIP H, VAHID S. Single-molecule optical spectroscopy [J]. Chemical Society Reviews, 2014, 43(4): 973-6.[9] HOUYU W, YANFENG Z, XIANGXU J, et al. Simultaneous capture, detection, and inactivation of bacteria as enabled by a surface-enhanced Raman scattering multifunctional chip [J]. Angewandte Chemie International Edition, 2015, 54(17): 5132-6.[10] BI L, RAO Y, QIN T, et al. Fabrication of large-scale gold nanoplate films as highly active SERS substrates for label-free DNA detection [J]. Biosensors & Bioelectronics, 2012, 43C(1): 193-9.[11] XU T T, HUANG J A, HE L F, et al. Ordered silicon nanocones arrays for label-free DNA quantitative analysis by surface-enhanced Raman spectroscopy [J]. Applied Physics Letters, 2011, 99(15): 153116--3.[12] QIAN X M, NIE S M. Single-molecule and single-nanoparticle SERS: from fundamental mechanisms to biomedical applications [J]. Chemical Society Reviews, 2008, 37(5): 912-20.[13] YU Y, LIN J, WU Y, et al. Optimizing electroporation assisted silver nanoparticle delivery into living C666 cells for surface-enhanced Raman spectroscopy [J]. Spectroscopy, 2011, 25(1): 13-21.[14] WANG A, RUAN W, SONG W, et al. Detection of the potential tumor marker of AFP using surface-enhanced Raman scattering-based immunoassay [J]. Journal of Raman Spectroscopy, 2013, 44(44): 1649-53.[15] JAMIL A K M, IZAKE E L, SIVANESAN A, et al. Rapid detection of TNT in aqueous media by selective label free surface enhanced Raman spectroscopy [J]. Talanta, 2015, 134C(732-8.[16] YANG H, YANG Y, LIU Z, et al. Self-assembled monolayer of NAD at silver surface: a Raman mapping study [J]. Surface Science, 2004, 551(s 1–2): 1-8.[17] CHANG J, CA?AMARES M V, AYDIN M, et al. Surface-enhanced Raman spectroscopy of indanthrone and flavanthrone [J]. Journal of Raman Spectroscopy, 2009, 40(11): 1557–63.[18] NIE S, EMORY S R. Probing single molecules and single nanoparticles by surface-enhanced Raman scattering [J]. science, 1997, 275(5303): 1102-6.[19] SHI Y E, LI L, YANG M, et al. A disordered silver nanowires membrane for extraction and surface-enhanced Raman spectroscopy detection [J]. Analyst, 2014, 139(10): 2525-30.[20] ? A S, ? J G, XIE W, et al. Surface-enhanced Raman spectroscopy in living plant using triplex Au Ag C core–shell nanoparticles [J]. Journal of Raman Spectroscopy, 2011, 42(4): 879-84.[21] SU Y-S, MANTHIRAM A. A new approach to improve cycle performance of rechargeable lithium–sulfur batteries by inserting a free-standing MWCNT interlayer [J]. Chemical Communications, 2012, 48(70): 8817-9.[22] LIU G, CAI W, LIANG C. Trapeziform Ag Nanosheet Arrays Induced by Electrochemical Deposition on Au-Coated Substrate [J]. Crystal Growth & Design, 2008, 8(8): 2748-52.[23] CHUANG Q, CHAO N, WENXUAN Y, et al. Highly-ordered, 3D petal-like array for surface-enhanced Raman scattering [J]. Small, 2011, 7(13): 1800-6.[24] HUANG Z, MENG G, HUANG Q, et al. Improved SERS performance from Au nanopillar arrays by abridging the pillar tip spacing by Ag sputtering [J]. Advanced Materials, 2010, 22(37): 4136-9.[25] LIU Y-J, ZHANG Z-Y, ZHAO Q, et al. The role of the nanospine in the nanocomb arrays for surface enhanced Raman scattering [J]. Applied Physics Letters, 2009, 94(3): 033103.[26] CUI Y, ZHENG X S, REN B, et al. Au@organosilica multifunctional nanoparticles for the multimodal imaging [J]. Chemical Science, 2011, 2(8): 1463-9.[27] HONGYAN L, ZHIPENG L, ZHUOXIAN W, et al. Enormous surface-enhanced Raman scattering from dimers of flower-like silver mesoparticles [J]. Small, 2012, 8(22): 3400–5.[28] CHENG L. Hierarchical silver mesoparticles with tunable surface topographies for highly sensitive surface-enhanced Raman spectroscopy [J]. Jmaterchema, 2014, 2(13): 4534-42.[29] ROBBIE K, BRETT M J. Sculptured thin films and glancing angle deposition: Growth mechanics and applications [J]. Journal of Vacuum Science & Technology A Vacuum Surfaces & Films, 1997, 15(3): 1460-5.[30] ZHOU Q, LI Z, YANG Y, et al. Arrays of aligned, single crystalline silver nanorods for trace amount detection [J]. Journal of Physics D: Applied Physics, 2008, 41(15): 152007.[31] ZHOU Q, YANG Y, NI J, et al. Rapid recognition of isomers of monochlorobiphenyls at trace levels by surface-enhanced Raman scattering using Ag nanorods as a substrate [J]. Nano Research, 2010, 3(6): 423-8.[32] HUANG J A, ZHAO Y Q, ZHANG X J, et al. Ordered Ag/Si nanowires array: wide-range surface-enhanced Raman spectroscopy for reproducible biomolecule detection [J]. Nano Letters, 2013, 13(11): 5039-45.[33] MESHIK X, WU X, ZHAO Y, et al. SERS spectrum of the peptide thymosin-β4 obtained with Ag nanorod substrate [J]. Journal of Raman Spectroscopy, 2014, 46(1): 194-6.[34] ZHOU Q, LI Z, NI J, et al. A Simple Model to Describe the Rule of Glancing Angle Deposition [J]. Materials Transactions, 2011, 52(3): 469-73.[35] ZHOU Q, LI Z, YANG Y, et al. Arrays of aligned, single crystalline silver nanorods for trace amount detection [J]. Journal of Physics D Applied Physics, 2008, 41(15): 152007.[36] ZHOU Q, YANG Y, NI J, et al. Rapid detection of 2, 3, 3′, 4, 4′-pentachlorinated biphenyls by silver nanorods-enhanced Raman spectroscopy [J]. Physica E: Low-dimensional Systems and Nanostructures, 2010, 42(5): 1717-20.[37] 周钦. 纳米银表面增强拉曼基底制备及其多氯联苯痕量检测应用 [D]; 清华大学, 2011.[38] ALARIFI H, HU A, YAVUZ M, et al. Silver Nanoparticle Paste for Low-Temperature Bonding of Copper [J]. Journal of Electronic Materials, 2011, 40(6): 1394-402.[39] JIANG Q, ZHANG S H, LI J C. Grain size-dependent diffusion activation energy in nanomaterials [J]. Solid State Communications, 2004, 130(9): 581-4.[40] MAHURIN S M, BAO L, DAI S. Controlled Layer‐by‐Layer Formation of Ultrathin Oxide Films on Silver Island Films for Surface‐Enhanced Raman Scattering Measurement [J]. Israel Journal of Chemistry, 2004, 76(15): 4531.[41] MA L, HUANG Y, HOU M, et al. Silver Nanorods Wrapped with Ultrathin Al2O3 Layers Exhibiting Excellent SERS Sensitivity and Outstanding SERS Stability [J]. Scientific Reports, 2015, 5(12890.[42] MA L, HUANG Y, HOU M, et al. Ag Nanorods Coated with Ultrathin TiO2 Shells as Stable and Recyclable SERS Substrates [J]. Scientific Reports, 2015, 5([43] MA L, WU H, HUANG Y, et al. High-Performance Real-Time SERS Detection with Recyclable Ag Nanorods@HfO2 Substrates [J]. Acs Applied Materials & Interfaces, 2016, 8(40): 27162.[44] HOU M, HUANG Y, MA L, et al. Compositional Analysis of Ternary and Binary Chemical Mixtures by Surface-Enhanced Raman Scattering at Trace Levels [J]. Nanoscale Research Letters, 2015, 10(1): 437.[45] 侯孟婧. 基于表面增强拉曼散射效应的痕量物质半定量与定量分析 [D]; 清华大学, 2016.[46] HOU M, HUANG Y, MA L, et al. Quantitative Analysis of Single and Mix Food Antiseptics Basing on SERS Spectra with PLSR Method [J]. Nanoscale Research Letters, 2016, 11(1): 1-8.