Abstract:The influence of liquid volume fraction changing with different sintering temperature and time on alloy microstructure and mechanical properties during sintering process with nominal composition Al–15Si–26Cu–057Mg was investigated. The results indicated that sintering at 560 ℃ by heating up under 10 ℃/min was the optimum temperature because that the volume fraction of 13% was benefit for alloy mechanical properties. The volume fraction of liquid phase began to stabilize after holding for 40 min at 560 ℃.The strength of alloy increased gradually with liquid phase distributing uniformly in the alloy by longer sintering time. Therefore sintering for 1 h at 560 ℃was the optimum condition. The dissolution of θ phase began around 500 ℃ and the dissolution of Q phase was around 510 ℃ to 535 ℃ during process of the temperature heating up so that the transformation temperature from solid phase to liquid phased creased by the dissolution of these phases with improving solid solubility of elements.
Yan M, Yu P, Schaffer G B, et al.Secondary phases and interfaces in a nitrogen-atmosphere sintered Al alloy: Transmission electron microscopy evidence for the formation of AlN during liquid phase sintering[J].Acta Materialia, 2010, 58(17):5667-5674
[4]
Matsuura K, Kudoh M, Kinoshita H, et al.Precipitation of Si particles in a super-rapidly solidified Al–Si hypereutectic alloy[J].Materials Chemistry and Physics, 2003, 81(2):393-395
[5]
Haris Rudianto S Y K N.MECHANICAL PROPERTIES OF Al-14Si-2.5Cu-0.5Mg[J].Rev.Adv.Mater.Sci, 2011, 28:145-149
[6]
Arribas I, Martín J M, Castro F.The initial stage of liquid phase sintering for an Al–14Si–25Cu–0.5Mg (wt%) PM alloy[J].Materials Science and Engineering: A, 2010, 527(16-17):3949-3966
[7]
Francisco M J M C.Sintering response & microstructural evolution of an Al-Cu-Mg-Si premix[J]., 2007, 43(6):59-69
[8]
H C. Neubing J G H D, Eds. H I S.. Advances in Powder Metallurgy and Particulate Materials[J]., 2002, :128-138
[9]
A Dudhmande T S M B.. Sintering and Properties of New P/M Aluminium Alloys and Composites[J]., 2005.[J].Metal Matrix Composites, 2005, :-
[10]
SCHAFFER G, HALL B, BONNER S, et al.The effect of the atmosphere and the role of pore filling on the sintering of aluminium , 2005, 54[J].Acta Materialia, 2006, 54(1):131-138
[11].
[12]
Su S S, Chang I T H, Kuo W C H.Effects of processing conditions on the sintering response of hypereutectic Al–Si–Cu–Mg PM alloys[J].Materials Chemistry and Physics, 2013, 139(2-3):775-782
[13]
Li Y J, Brusethaug S, Olsen A.Influence of Cu on the mechanical properties and precipitation behavior of AlSi7Mg05 alloy during aging treatment[J].Scripta Materialia, 2006, 54(1):99-103
[14]
Heard D W, Donaldson I W, Bishop D P.Metallurgical assessment of a hypereutectic aluminum–silicon PM alloy[J].Journal of Materials Processing Technology, 2009, 209(18-19):5902-5911
[15]
CHAKRABARTI D J L D E.Phase relations and precipitation in AI—Mg—Si alloys with Cu additions[J].Progress in Materials Science, 2004, 49(3):389-410
Keong K G, Sha W, Malinov S.Computer modelling of the non-isothermal crystallization kinetics of electroless nickel–phosphorus deposits[J].Journal of Non-Crystalline Solids, 2003, 324(3):230-241
[23]
QU S J, FENG A H, GENG L, et al.DSC analysis of liquid volume fraction and compressive behavior of the semi-solid Si3N4wAl–Si composite[J].Scripta Materialia, 2007, 56(11):951-954