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10 June 2026, Volume 36 Issue 03
    

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    Experts Forum
  • ZHAO Dingguo, LIANG Kuan, WANG Shuhuan, WANG Baohua, WANG Shizhao, XUE Yuekai
    Powder Metallurgy Industry. 2026, 36(03): 1-16. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240225
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    【Objective】 In response to the application requirements of additive manufacturing (AM) technology for metallic lattice-structured components, this paper clarifies the key technical points and research progress of AM in fabricating metallic lattice structures, investigates the critical issues in the forming, property regulation and defect control of such components, and provides theoretical references and research insights for the technological development and engineering application of additively manufactured metallic lattice-structured components.
    【Method】 Using literature investigation and comprehensive analysis, this work systematically reviews the development history and application status of additively manufactured metallic lattice-structured components, focuses on the classification and characteristics of lattice structures, and expounds the technical advantages of additive manufacturing for fabricating lattice structures. From a metallurgical perspective, it analyzes the dynamic process of powder melting and solidification during the lattice structure forming procedure, investigates the regulation mechanism of heat treatment on the mechanical properties of the components, comprehensively summarizes the defect formation mechanisms of metallic lattice structures, and sorts out the mainstream defect detection methods at the current stage.
    【Result】 The structural characteristics and differences in mechanical properties of three types of lattice structures (truss-type, triply periodic minimal surface (TPMS), and bionic-type lattices) are clarified. Additive manufacturing is confirmed to exhibit prominent advantages in the fabrication of metallic components with complex lattice structures, such as high design flexibility, large forming freedom, and the ability to realize the synergistic optimization of lightweight and performance. The influence laws of micro-melt pool characteristics, remelting phenomena and process parameters on the forming quality of lattice structures are revealed. The coupling relationships between heat treatment processes, microstructures and mechanical properties of lattice structures with different matrix materials are analyzed. The common defects and corresponding formation mechanisms of additively manufactured metallic lattice-structured components are summarized, and industrial computed tomography (CT) integrated with intelligent algorithms is identified as an efficient approach for the defect detection of lattice structures at the current stage.
    【Conclusion】 Additive manufacturing provides an effective approach for the fabrication of complex metallic lattice structures. Benefiting from the advantages of high specific strength, high specific stiffness, lightweight and multifunctionality, metallic lattice‑structured components present broad application prospects in aerospace, medical treatment, automotive engineering and other fields. Among these aspects, the regulation of the melting and solidification process during additive manufacturing, the optimization of heat treatment processes, and defect detection and control are the key links to improve the forming quality and performance of additively manufactured metallic lattice‑structured components. For the future development of additive manufacturing technology for metallic lattice‑structured components, efforts should be focused on the multi‑scale optimal design of lattice structures, the investigation of the metallurgical essence of additive manufacturing, the construction of the full‑cycle manufacturing process, and the full exploitation of AM technical advantages, so as to promote the engineering application of this technology in high‑end equipment manufacturing and other fields.
  • Research and Development
  • SONG Runhua, SHI Songyi, YANG Yajin, WU Can, LI Dongfeng, SHI Rongpei, QIN Hailong
    Powder Metallurgy Industry. 2026, 36(03): 17-24. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240215
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    【Objective】 This study aims to investigate the constitutive behavior of solution-treated FGH95 nickel-based superalloy during the continuous cooling process, with a focus on the precipitation of the secondary γ' phase and its influence on mechanical properties. The objective is to clarify the relationship between thermal history, γ' precipitation evolution, and mechanical response, and to establish a constitutive model capable of describing the material behavior during non-isothermal cooling.
    【Method】 Solution-treated FGH95 alloy specimens were prepared by holding at 1 180 ℃, cooling uniaxial tensile tests were conducted under two different thermal paths, namely direct heating from room temperature and cooling interruption from the solution temperature, at temperatures ranging from room temperature to 1 000 ℃. Tension-compression cyclic tests were also performed to investigate the hardening behavior. Microstructural characterization was carried out using scanning electron microscopy under different cooling rates. Thermodynamic calculations and precipitation simulations were performed using JMatPro and MatCalc to analyze phase evolution. Based on experimental observations, a constitutive model incorporating dislocation slip resistance and precipitation strengthening was established, in which the evolution of the secondary γ' phase volume fraction was described by the JMA equation. Model parameters were calibrated by fitting experimental stress-strain curves.
    【Result】 The results show that γ' phase precipitation during continuous cooling at 20 ℃/min is inevitable and mainly occurs within a high-temperature range. Compared with the direct heating condition, the specimens subjected to cooling exhibit higher yield strength and strain hardening rate at the same temperature. This difference is caused by the distinct thermal histories prior to deformation, which result in different stages of secondary γ' precipitation. During cooling from 1 180 ℃, a significant amount of secondary γ' phase has already precipitated before deformation, whereas only limited precipitation occurs during heating from room temperature. In addition, the precipitation of γ' phase continues during deformation at elevated temperatures, further enhancing strain hardening. Microstructural observations confirm that lower cooling rates promote the formation of coarser γ' precipitates, while higher cooling rates lead to finer and more densely distributed secondary γ' particles. The proposed constitutive model accurately captures the evolution of flow stress under both heating and cooling conditions and reflects the contribution of precipitation strengthening.
    【Conclusion】 The constitutive behavior of solution-treated FGH95 superalloy during continuous cooling is strongly dependent on the evolution of the secondary γ' phase. The difference in mechanical properties between heating and cooling conditions originates from the distinct precipitation states induced by thermal history. The developed constitutive model, which incorporates precipitation evolution based on the JMA framework, can effectively predict the mechanical response during continuous cooling and provides a useful tool for analyzing microstructure-property relationships and optimizing heat treatment processes.
  • LI Dongli, CHEN Hongsheng, DONG Shengzhi, ZHOU Mingge, WANG Fanggui, XU Jiyuan, DU Jingtao
    Powder Metallurgy Industry. 2026, 36(03): 25-32. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250203
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    【Objective】 Containing 60% Ce magnets were subjected to grain boundary diffusion(GBD)treatment using Pr70Al20Co10 alloy as the diffusion source. The purpose is providing both theoretical and experimental foundations for the preparation of low-cost, high-performance Ce-based magnets.
    【Method】 The diffusion source was placed at both ends of the substrate to be diffused using the patch method, and heat treatment was carried in a vacuum sintering furnace. The magnetic properties of the magnets before and after diffusion treatment were tested using a MIN-6000C instrument. Composition analysis was performed via inductively coupled plasma optical emission spectrometry (ICP-OES). The microstructure and morphology of the magnets were observed using a field emission scanning electron microscope (SEM). The elemental distribution in the magnets was analyzed in detail with an electron probe microanalyzer (EPMA). X-ray diffraction (XRD) was employed to analyze the diffraction patterns. Thermogravimetric-differential thermal analysis (TG-DTA) was conducted to determine the Curie temperature (Tc).
    【Result】 (1) After diffusion for 6-12 h, the Hcj of Ce60 magnets significantly improves, while the Br remains essentially unchanged. Among these, the magnet diffused for 8 h exhibits the greatest performance enhancement: Hcj increases from 6.51  kOe to 10.61  kOe, an improvement of ~63%, while Br slightly decreases from 11.12  kGs to 11.05  kGs, a reduction of ~0.6%. After diffusion treatment, the absolute values of both βHcj and αBr are higher than those of the original magnet. (2) After diffusion treatment, the crystal structure of the main phase in the magnet remains unchanged, and no new phases are formed.
    【Conclusion】 (1) As the diffusion time increases, the Hcj of the magnet initially increases and then decreases. The magnet subjected to 8 hours of diffusion exhibits the greatest improvement in coercivity, the Hcj of the Ce60 magnet is enhanced from 6.51 kOe to 10.61 kOe, an increase of 4.1 kOe, achieving a remarkable improvement of ~63%. Within the temperature range of 20~80 ℃, compared to the undiffused magnet, the βHcj of the diffused magnet decreases slightly, while the αBr remains almost unchanged. (2) Electron Probe Microanalysis (EPMA) and Backscattered Electron (BSE) imaging reveal that Pr and Co are predominantly concentrated in the grain boundary phase after diffusion. A small amount of Pr diffuses into the main phase, forming a core-shell structure. Al is generally uniformly distributed throughout the magnet, with a minor fraction enriched in the grain boundaries. Thermo gravimetric analysis (TGA) indicates that the Curie temperature (Tc) of the as-prepared Ce60 magnet is approximately 230 ℃, and the Tc remains nearly unchanged after the diffusion treatment. The significant enhancement in the coercivity of the Ce60 magnet is primarily attributed to two factors: the reduced aggregation of Ce at the grain boundaries and the formation of a continuous, uniform thin rare earth-rich phase surrounding the main phase grains.
  • CAO Rui, LÜ Shiya, MENG Lingbing, MA Hongqiu, ZHAO Gang
    Powder Metallurgy Industry. 2026, 36(03): 33-39. https://doi.org/10.13228/j.boyuan.issn1006-6543.20260060
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    【Objective】 Iron-based amorphous soft magnetic alloys are widely applied in high-frequency electronic devices and power energy storage systems owing to their low loss and high permeability. Nevertheless, conventional iron-based alloys exhibit poor amorphous forming ability, high high-frequency eddy current loss and inferior DC bias resistance, limiting their large-scale engineering promotion. To address these shortcomings and improve the comprehensive soft magnetic properties of FeSiBC alloys, partial Fe substitution by P was adopted for structural modification, aiming to enhance the amorphous forming performance, high-frequency magnetic stability and anti-DC bias capability of the alloys.
    【Method】 Spherical FeSiBCP soft magnetic alloy powders were fabricated by a gas-water combined atomization process using high-purity industrial iron, silicon, ferroboron, carbon flakes and ferrophosphorus. The raw materials were melted at 1 600 ℃, then poured at 1 500 ℃. The molten steel was atomized into fine spherical droplets via gas-water synergy, followed by rapid condensation, dehydration, drying and screening. The obtained powders were blended with insulating glue, compacted, cured and wound with copper wires to prepare magnetic core samples with an effective cross-sectional area of 0.1 cm2.
    【Result】 The gas-water combined atomization process can stably prepare FeSiBCP alloy powders with high sphericity and uniform particle size, featuring good process stability. With the increase of P atomic fraction, the alloy microstructure gradually transforms from crystalline to amorphous state. When the P atomic fraction is 4 at.%, the Fe(SiBC)P alloy realizes complete amorphization, and its coercivity is significantly reduced. In the frequency range of 100~1 000 kHz, the optimized alloy magnetic core delivers an excellent effective permeability of 20.13 and superior high-frequency stability. Moreover, it retains a permeability retention rate of 77.3% under a DC bias field of 100 Oe, showing outstanding anti-DC bias performance. Moderate P doping optimizes the amorphous microstructure of the alloy, which effectively reduces the coercivity, eddy current loss and high-frequency total iron loss of the magnetic powder core.
    【Conclusion】 P element modification can effectively improve the amorphous forming ability of FeSiBC alloys and optimize their comprehensive soft magnetic properties. The optimized Fe(SiBC)P amorphous magnetic powder core has excellent high-frequency stability and prominent anti-DC bias performance, which is well applicable to working conditions with high frequency and large DC bias field. The gas-water combined atomization process has good repeatability and batch preparation capability. This study provides a reliable theoretical basis and technical reference for the industrialized production and engineering application of high-performance iron-based amorphous soft magnetic powder cores.
  • XIN Bowen, JIN Hui, LI Chengwei, WANG Yiyong, ZHANG Yangrong
    Powder Metallurgy Industry. 2026, 36(03): 40-45. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240193
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    【Objective】 The objective of this study was to purify copper oxide from electronic industrial waste, prepare ultrafine copper powder by hydrogen reduction, and analyze the effects of reduction temperature and reduction time on the micro morphology, particle size and specific surface area of ultrafine copper powder, so as to determine the optimal preparation process conditions.
    【Method】 First, copper oxide from electronic industrial waste was purified. Then, the treated copper oxide powder was subjected to high-energy ball milling to obtain a copper oxide powder precursor. Ultrafine copper powder was prepared by hydrogen reduction. The micro morphology of the ultrafine copper powder was observed by scanning electron microscope, and its particle size and specific surface area were detected by laser particle size analyzer. Finally, combined with the experimental data, the effects of reduction temperature and reduction time on the micro morphology, particle size and specific surface area of ultrafine copper powder were analyzed.
    【Result】 The experimental results show that the optimal process conditions for preparing ultrafine copper powder are ball milling to an average particle size of 0.18 μm, reduction temperature of 600 ℃, reduction time of 60 min, and hydrogen flow rate of 0.5 L/min. Under these conditions, the average particle size of the obtained copper powder is 8.72 μm, the reduction rate reaches 99.7%, the reduction degree is high, and the powder surface is smooth and not easy to oxidize. The particle size of copper powder increases with the increase of reduction temperature and the extension of reduction time.
    【Conclusion】 The purification of copper oxide from electronic industrial waste combined with high-energy ball milling and hydrogen reduction is an effective method to prepare ultrafine copper powder. The optimal process conditions determined in this study can obtain high-quality ultrafine copper powder with high reduction rate, smooth surface and good anti-oxidation performance. The reduction temperature and reduction time are key factors affecting the particle size of ultrafine copper powder, specifically, higher reduction temperature and longer reduction time will lead to larger particle size of copper powder.
  • YE Jianlin, SUN Yang, YANG Xiaoxiao, GAO Ling, ZHANG Weigang, LIU Lu
    Powder Metallurgy Industry. 2026, 36(03): 46-54. https://doi.org/10.13228/j.boyuan.issn1006-6543.20260025
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    【Objective】 With the continuous progress of aerospace, nuclear energy and other high-end strategic industries, additive manufacturing and other advanced forming technologies put forward stricter demands for the overall performance of refractory metal raw powder. High-sphericity, good-fluidity and high-apparent-density molybdenum powder is the key foundation for high-quality forming of molybdenum alloy parts. To solve the bottleneck of high-performance spherical molybdenum powder mass preparation, this work aims to adopt DC arc plasma spheroidization technology to modify commercial irregular molybdenum powder, explore the influence rules of key process parameters on powder comprehensive performance, and reveal the intrinsic spheroidization mechanism, so as to provide technical basis for industrial mass production and high-end engineering application of spherical molybdenum powder.
    【Method】 Commercial irregular molybdenum powder was selected as the experimental raw material, and DC arc plasma spheroidization equipment was used for powder modification treatment. Focusing on two critical process parameters including powder feeding rate and plasma power, comparative experiments with different parameter combinations were carried out. Multiple testing devices were applied for multi-dimensional characterization: scanning electron microscope was used to observe powder microscopic morphology, X-ray diffraction was adopted to analyze phase composition changes, and special testing instruments were utilized to detect particle size distribution, powder flowability and apparent density of samples before and after spheroidization.
    【Result】 DC arc plasma treatment would not change the phase structure of molybdenum powder, and the spheroidized powder still presents single body-centered cubic molybdenum phase without oxide impurities or miscellaneous phases. The optimal process parameters are determined as powder feeding rate of 80 g/min and plasma power of 45 kW. Under this condition, the powder spheroidization rate is over 98%, with smooth particle surface and no obvious agglomeration. Compared with raw powder, the particle size distribution become more uniform, the median particle size decreases from 34.47 μm to 23.56 μm. Meanwhile, the powder flowability and apparent density are greatly improved, among which the flowability is optimized to 11.6 s/50g, and the apparent density increased by 117.9%.
    【Conclusion】 DC arc plasma technology is highly applicable and reliable for the spheroidization modification of molybdenum powder. The whole spheroidization process can be summarized as three stages of energy absorption, droplet formation and solidification stabilization. Excessively high plasma power will induce nanoparticle coating on powder surface, which has potential application value in functional modification. The optimized process parameters obtained in this study can effectively improve the sphericity, flowability and bulk density of molybdenum powder, which is conducive to the popularization and application of high-performance spherical molybdenum powder in advanced powder forming fields.
  • GAI Xin, CHEN Haohan, ZHU Yonghui, GONG Ya, JIANG Wentian, DING Tao, Fu Chao
    Powder Metallurgy Industry. 2026, 36(03): 55-60. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250201
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    【Objective】 In the field of metal additive manufacturing, the properties of raw material powders are one of the key factors affecting the quality of printed parts. Ti31 titanium alloy is a Ti-Al-Mo-Ni based near α titanium alloy with high-temperature resistance, corrosion resistance, and hydrogen embrittlement resistance, which has been widely applied in marine engineering and nuclear industries. However, at present, there are relatively few research on the preparation of Ti31 titanium alloy powders and the performance of printed sample. Therefore, it is necessary to conduct relevant research to clearly explain the effect of powder preparation methods on Ti31 alloy powders and printed parts.
    【Method】 Ti31 titanium alloy powders were prepared by electrode induction gas atomization (EIGA) and plasma rotating electrode process (PREP), respectively. The characteristics of powders including chemical composition, morphology, particle size distribution of EIGA and PREP powders were compared. The vibration sieving method was used to classify the particle size of the obtained powder under inert gas protection, and Ti31 powder with a particle size of 15-53 μm was obtained after sieving. The selective laser melting (SLM) adaptability of the powders was analyzed.Ti31 samples were prepared using with MT-450 equipment and TC4 titanium alloy as the printing substrate. The substrate surface was cleaned and dried before printing. The forming scanning strategy was strip scanning, with adjacent layers rotated 67 °. The Ti31 printed samples were solution treatmented, with a process of holding at 800 ℃ for 2 hours and then air cooling to room temperature.SLM printed samples were subjected to chemical composition testing and morphology obcevation after polishing. Tensile tests of Ti31 printed samples after heat treatment were conducted at room temperature, with the tensile samples taken from the X forming direction.
    【Result】 The results show that the Ti31powder produced by two methods exhibit low non-metallic element content, and the main phase of the powders is α-Ti hexagonal close-packed (hcp) crystal structure. Furthermore, compared with EIGA powder, the PREP powder exhibits lower oxygen content, higher sphericity, better flowability, and lower hollow powder rate. The main phase of Ti31 powder prepared by EIGA method and PREP method is α-Ti hcp crystal structure.The chemical composition and tensile properties at room temperature of the printed Ti31 alloy meet the requirements of Ti31 forging standard. The EIGA-fabricated specimens exhibit higher ultimate tensile strength and yield strength, while the PREP-fabricated specimens show superior elongation and reduction.
    【Conclusion】 The Ti31 powder prepared by EIGA and PREP methods was subjected to SLM additive testing, and the room temperature tensile properties of the Ti31 printed samples met the performance indicators of Ti31 forging samples, verifying the good compatibility between Ti31 powder and SLM process.
  • YU Yongliang, YANG Shanying, ZHANG Yi, WANG Yankang, LI Guoping, LI Songlin
    Powder Metallurgy Industry. 2026, 36(03): 61-68. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250047
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    【Objective】 The 316L stainless steel is a crucial engineering material, widely used in the manufacturing of wear-resistant and corrosion-resistant components. In order to further enhance the performance of 316L powder metallurgy steel, nitrogen, showing strong strengthening effect on powder metallurgy components, was added to the powder metallurgy stainless steel to improve its microstructure and material properties.
    【Method】 In this paper, the 316L nitrogen-containing powder metallurgy stainless steel was prepared by PM techniques with Cr2N additive as a nitrogen resource, then, the microstructure and performance of PM 316L nitrogen-containing stainless steel were studied.
    【Result】 Results show that the grain size of 316L nitrogen-containing stainless steel reduces gradually, and the particle shape becomes round with continued increase of N content regardless of as-sintered state or as-heat treated state, large size of blocky and banding particles are observed with further increase of N content. Results of mechanical properties indicate that the hardness of 316L nitrogen-containing stainless steel increases monotonously with the increase of N content, and the hardness of 316L nitrogen-containing stainless steel as-sintered state and as-heat treated state is 75.4HRB and 90.2HRB respectively at the designed N content 1.5%. The tensile strength of 316L nitrogen-containing stainless steel increases firstly and then decreases with the increase of N content, in addition, the tensile strength of PM 316L nitrogen-containing as-heat treated state is superior to that of the samples as-sintered state, while the tensile strength of PM 316L nitrogen-containing as-sintered state and as-heat treated state reaches maximum value 518.3 MPa and 597.1 MPa respectively at N content 0.9%. The impact toughness of 316L nitrogen-containing stainless steel as-sintered state changes little when the designed N content is no more than 0.9%. However, the value of impact toughness decreases remarkably with the continuously increased N content. The impact toughness of the 316L nitrogen-containing stainless steel as-heat treated state is inferior to that of the as-sintered stainless steel. The impact toughness of the 316L nitrogen-containing stainless steel as-heat treatment state increases slightly at 0.3% N designed content, subsequently, it decreases monotonously with the increase of N content and desreases abruptly when designed N content exceeding 0.9%.
    【Conclusion】 The nitrogen content in PM stainless steel was retained only 25%~30% for high volatility of nitrogen element, however, even a small quantity of nitrogen has an excellent strengthening effect on properties of PM 316L steel, so it is a feasible method to manufacture high-performance PM 316L steel with nitrogen element additive.
  • LIN Xiaohui, XUE Jianrong, HUANG Li, CHANG Tian, LIANG Jing, ZHANG Wen
    Powder Metallurgy Industry. 2026, 36(03): 69-75. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240217
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    【Objective】 Molybdenum is a typical metal exhibiting a ductile-brittle transition phenomenon, with its ductile-brittle transition temperature generally ranging from 200 ℃ to 300 ℃. Therefore, it is prone to unforeseen brittle fracture during service at room temperature. The addition of rhenium (Re) to molybdenum can significantly reduce its ductile-brittle transition temperature while improving the strength of molybdenum alloys. There are various testing methods for ductile-brittle transition temperature, and the results obtained by different methods may vary. The variability in testing poses challenges for cross-comparisons, material selection, and engineering applications of molybdenum alloy ductile-brittle transition temperatures. This paper investigates the ductile-brittle transition phenomenon of Mo-14Re alloy under different testing conditions, providing a reference for the design and application of Mo-Re alloys.
    【Method】 Mo-14Re sintered billets were obtained by cold isostatic pressing and high temperature hydrogen sintering at 2 100 ℃. Mo-14Re bars with a diameter of ϕ20 mm were obtained by multi pass high temperature forging of sintered billets at high temperature. Mo-14Re bars were sampled along the axial direction after vacuum heat treatment at 900 ℃/1 h. The ductile-brittle transition temperature of Mo-14Re alloy was measured by three-point bending method, impact toughness method and tensile method. The test temperatures are -120 ℃, -140 ℃, -160 ℃, -180 ℃ and -196 ℃ respectively, and at least three samples are tested under each condition. The low temperature environment required for the test is obtained by the mixture of liquid nitrogen and alcohol. After the test, the tensile and impact fracture surfaces were taken and the fracture morphology was observed by SEM.
    【Result】 During the three-point bending test, the bending strength of the alloy increases gradually with the test temperature decreasing from -140 ℃ to -196 ℃, and brittle fracture occurs at -196 ℃. At -196 ℃, the fracture mode of the alloy changes from toughness to brittleness with the increase of loading rate from 0.5 mm/min to 2.0 mm/min. During the tensile process, the tensile strength of the alloy increases from 942 MPa to 1055 MPa with the test temperature decreasing from -120 ℃ to -196 ℃. The elongation after fracture decreases sharply to 1.6% at -196 ℃, and there is almost no plastic deformation before fracture. The fracture morphology shows that the alloy has ductile-brittle transition at -180~-196 ℃. During the impact test, the impact toughness of the alloy decreased with the decrease of the test temperature. At -196 ℃, the impact toughness decreased sharply to 3.05 J/cm2, which obviously deviated from the linear trend of the impact toughness with the decrease of temperature in the range of -140~-180 ℃.
    【Conclusion】 The ductile-brittle transition temperatures of Mo-14Re alloy bars tested by three-point bending method, tensile method and impact method are all in the range of -180~-196 ℃. With the decrease of temperature, the bending strength and tensile strength of Mo-14Re alloy increase, while the impact toughness and plastic deformation ability decrease. The low temperature results in the decrease of dislocation mobility and the decrease of crystal planes for sliding, which increases the strength and decreases the plasticity of Mo-14Re alloy, resulting in ductile-brittle transition. At the same test temperature, the change of strain rate is one of the key factors affecting the ductile-brittle transition temperature of Mo-14Re alloy.
  • YIN Yi, WANG Tiejun, QIN Sigui, SHI Yingli, YU Hongxin, XU Shiwei
    Powder Metallurgy Industry. 2026, 36(03): 76-83. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240076
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    【Objective】 Tungsten (W) is considered one of the most promising candidates for plasma-facing materials (PFMs) in fusion reactors due to its high melting point, excellent sputtering resistance, low deuterium-tritium retention, and high thermal conductivity. However, several drawbacks of tungsten, including low-temperature brittleness, irradiation embrittlement, and recrystallization embrittlement, severely restrict its engineering applications. This study aims to fabricate a fine-grained W alloy by powder metallurgy and hot rolling with 0.5wt.% Hf addition, investigate its microstructure, high-temperature mechanical properties, and thermal stability, and reveal the strengthening mechanism of Hf in W matrix.
    【Method】 Pure W powder and HfH₂ powder were used as raw materials to prepare pure W (PW) and W-0.5% Hf alloy. The mixed powders were ball-milled in argon atmosphere for 4 h with a ball-to-powder ratio of 8:1 and a rotating speed of 300 r/min. The green compacts were obtained by cold isostatic pressing at 200 MPa for 5 min, followed by sintering at 2 300 ℃ for 7 h in hydrogen atmosphere. The sintered bulks were rolled with five passes at 1 400-1 600 ℃ with a total deformation of ~68%, and then annealed at 1 100 ℃ for 60 min to release residual stress. The recrystallization temperature was evaluated by isochronal annealing at 1 200-1 600 ℃ for 1 h. The density was measured by the Archimedes method, and microhardness was tested by Vickers indentation. High-temperature tensile tests were carried out at 100-1 000 ℃ in vacuum. Microstructure was characterized by optical microscope (OM), scanning electron microscope (SEM) equipped with energy dispersive spectrometer (EDS), and transmission electron microscope (TEM).
    【Result】 The relative densities of pure tungsten (PW) and W-0.5%Hf alloy are both approximately 99.4%, and Hf addition has no obvious effect on densification. Compared with pure tungsten, the W-0.5 Hf alloy possesses finer fibrous grains and higher Vickers hardness. Uniformly dispersed nanoscale second-phase particles are observed in the alloy, which are identified as monoclinic hafnium oxide (HfO₂) by EDS and selected area electron diffraction (SAED). High-temperature tensile results demonstrate that W-0.5% Hf exhibits superior strength and plasticity over pure tungsten at all tested temperatures. At 100 ℃, the ultimate tensile strength (UTS) reaches (1 008±7.09) MPa, which is 14.5% higher than that of pure tungsten. At 200 ℃, the total elongation (TE) is 9.15%±0.77%, with an increase of 80.8%. At 1 000 ℃, the UTS still remains at (466.64±7.63) MPa. Fracture morphology reveals that the alloy is dominated by transgranular cleavage fracture at low temperatures and transforms into typical ductile fracture at high temperatures, with HfO₂ particles distributed at the center of dimples. The recrystallization temperature of pure tungsten is about 1 200 ℃, while that of the W-0.5% Hf alloy increases to 1 400 ℃, and HfO₂ particles effectively pin grain boundaries and inhibit grain growth during annealing.
    【Conclusion】 Hf introduced by HfH₂ reacts with impurity oxygen at W grain boundaries to form thermally stable HfO₂ nanoparticles, which purifies and strengthens grain boundaries. The nano HfO₂ particles pin dislocations and grain boundaries, leading to grain refinement and dispersion strengthening. As a result, W-0.5 Hf alloy presents significantly improved tensile strength and ductility compared with pure W, especially the elongation is greatly enhanced at medium temperatures. Meanwhile, the pinned grain boundaries effectively inhibit recrystallization and grain growth, raising the recrystallization temperature by about 200 ℃ and improving high-temperature stability. This hot-rolled W-0.5%Hf alloy with fine grains, high strength, good ductility, and elevated recrystallization temperature provides a promising candidate for high-performance plasma-facing materials in nuclear fusion reactors.
  • LIU Ning, YU Yong, WANG Xiao, LI Dongyang
    Powder Metallurgy Industry. 2026, 36(03): 84-91. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240221
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    【Objective】 This study aimed to investigate the effects of powder loading on the rheological behavior of wax-based feedstocks and the as-sintered density of NiTi shape memory alloys fabricated by metal injection molding (MIM), in order to identify an optimal powder loading for defect-free molding and high densification.
    【Method】 Gas-atomized pre-alloyed NiTi powder (Ni50.47Ti49.53, at%) with a median particle size of 11.8  μm was mixed with a wax-based binder system consisting of 60% paraffin wax, 40% polypropylene, and a minor amount of stearic acid. Three feedstock formulations with powder loadings of 55 vol% (TN55), 60 vol% (TN60), and 65 vol% (TN65) were prepared by mixing under argon protection at 160-180 ℃ for 3 hours. Rheological properties were evaluated using a capillary rheometer at temperatures of 150  ℃, 170  ℃, and 190  ℃ across shear rates ranging from 100 to 1 200 s-1. The viscosity data were employed to calculate the power-law exponent n (strain sensitivity), the viscous flow activation energy E (temperature sensitivity), and the comprehensive rheological factor α~STV~. Green parts were injection-molded, subjected to solvent debinding in dichloromethane at 38  ℃ for 12  h, thermally debound in flowing argon at 600  ℃, and finally sintered in vacuum (10-4  Pa) at 1 240  ℃ for 6  h with a heating rate of 5  ℃/min. Weight loss during solvent debinding, carbon and oxygen contents after thermal debinding and sintering, defect rates, and sintered relative densities were systematically recorded and analyzed.
    【Result】 The viscosity of all feedstocks decreases monotonically with increasing temperature and shear rate, exhibiting typical pseudoplastic behavior. The TN60 feedstock exhibits the highest strain sensitivity with a lower power-law exponent *n* value (approximately 0.51-0.55), indicating better fluidity and shear-thinning response under identical external shear conditions. In contrast, higher powder loadings result in higher viscous flow activation energy E values, TN65 possesses E values around 42.76 kJ·mol-1 at low shear rates, implying greater temperature sensitivity and potential viscosity variation within the mold cavity. The comprehensive rheological factor α~STV~, which integrates viscosity, temperature sensitivity, and strain sensitivity, is largest for the TN65 feedstock (207.86 at low shear rate and 352.76 at high shear rate), demonstrating its superior overall rheological performance among the three formulations. During solvent debinding, the weight loss of TN65 reaches approximately 4.15% after 12 h, approaching the theoretical maximum of 4.186% based on the wax content. After thermal debinding, the TN65 feedstock achieves the highest yield of defect-free parts (99.8%), with negligible cracks or bubbles observed. The carbon and oxygen impurity contents after sintering are not significantly influenced by powder loading and are primarily controlled by process optimization, post-sintering oxygen and carbon contents are as low as 0.16 wt% and 0.03 wt%, respectively, representing a substantial reduction compared with previous studies. Sintered density increases markedly with powder loading, from 92.4% for TN55 to 94.4% for TN60 and finally 96.7% of theoretical density for the TN65 feedstock. The higher green density associated with increased powder loading promotes more effective pore elimination and interparticle bonding during solid-state sintering of the pre-alloyed powder.
    【Conclusion】 A powder loading of 65 vol% is the optimal design for MIM NiTi alloys fabricated with the wax-based binder system. This formulation provides the best comprehensive rheological stability, minimizes molding defects during injection, and yields the highest sintered density (96.7%) with low interstitial impurity levels, thereby facilitating the production of high-performance NiTi shape memory components with improved mechanical integrity and dimensional precision.
  • HU Bin, LAI Yunjin, WANG Dongdong, LIU Xiaofei, WANG Yongzhe, WANG Kai
    Powder Metallurgy Industry. 2026, 36(03): 92-99. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250060
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    【Objective】 This study aims to address the critical issue of microcrack formation during the selective laser melting (SLM) of GH3230 superalloy. The primary objective is to optimize the SLM process parameters and systematically investigate the synergistic effects of hot isostatic pressing (HIP) and subsequent heat treatment (HT) on the microstructure evolution and mechanical properties of the alloy, thereby providing a feasible processing strategy for the high-quality SLM formation of GH3230 superalloy.
    【Method】 Spherical GH3230 superalloy powder prepared via the high-speed plasma rotating electrode process (SS-PREP) was used as the raw material. The SLM process was conducted by adjusting the laser power to screen the optimal parameters with minimal microcracks. Three groups of samples were prepared: as-SLM, HIP-treated, and HIP+HT-treated. The microstructures were characterized using optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction (XRD). The mechanical properties were evaluated by tensile tests at both room and high temperatures, and the fracture mechanisms were analyzed via fractography.
    【Result】 Low laser power results in insufficient energy density and subsequent lack-of-fusion defects, while the parameter of 205 W effectively reduces microcracks and eliminates unmolten defects. After HIP treatment, all microcracks in the as-SLM state are fully closed. Chain-like carbides are precipitated continuously along both grain boundaries and intragranular regions, with an average size of 1.31 μm and an equivalent grain diameter of 7.14 μm. Following HIP+HT treatment, the carbides underwent remelting and redistribution, reducing their average size to 1.18 μm, while the grain size increases by 32.1% compared to the HIP state. This microstructural evolution lead to a decrease in room-temperature tensile strength due to the weakening of precipitate strengthening, but a synergistic enhancement in high-temperature tensile strength and plasticity is achieved via refined grain boundary carbides and grain coarsening. Fracture analysis reveals that the HIP+HT state exhibites quasi-cleavage fracture at room temperature and ductile fracture at high temperatures.
    【Conclusion】 The 205 W laser power parameter effectively mitigates microcrack and lack-of-fusion defects in SLM-fabricated GH3230 superalloy. HIP treatment achieves full crack closure and uniform carbide precipitation, while HIP+HT further optimizes the microstructure by regulating carbide distribution and grain growth. The HIP+HT-treated alloy exhibits a balanced combination of reduced room-temperature strength and improved high-temperature mechanical properties, which is attributed to the cooperative effects of refined carbides and grain coarsening. These findings provide critical technical guidance for the industrial application of SLM-fabricated GH3230 superalloy in high-temperature service environments.
  • LIU Jianxiu, WANG Hao, CHEN Yang, JIANG Aiyun, DOU Qianchao, ZHOU Yajun
    Powder Metallurgy Industry. 2026, 36(03): 100-106. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240107
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    【Objective】 This study aims to systematically investigate the effect of alumina whisker content on the friction and wear properties of copper-based friction materials, clarify the evolution law of hardness, density, friction coefficient and wear rate with whisker addition, and reveal the corresponding wear mechanism transformation, so as to provide experimental support and theoretical reference for optimizing the composition and performance of copper-based powder metallurgy friction materials.
    【Method】 Copper-based friction materials reinforced with 0、0.25、0.50, 0.75 wt% alumina whiskers were prepared by powder metallurgy including cold pressing and vacuum hot‑press sintering. The hardness and density were measured by Brinell hardness tester and Archimedes drainage method. The friction and wear tests were carried out on an MM3000 tester under braking speeds of 150-350 km/h to obtain friction coefficient and wear mass loss. The microstructure and worn surface morphology were observed by scanning electron microscopy (SEM) to analyze the dispersion state of whiskers and wear characteristics.
    【Result】 The hardness first increases and then decreases with the rise of alumina whisker content, reaching the maximum at 0.25 wt%, while the density decreases linearly. At 0.25 wt% alumina whiskers, the friction coefficient increases by about 3% and the wear mass loss decreases by about 5% compared with the unreinforced sample. As the whisker content further increases, both friction coefficient and hardness decline, whereas wear loss increases obviously. SEM observations show that appropriate alumina whiskers disperse uniformly and reduce spalling pits and cracks. With increasing content, whisker agglomeration occurres, causing interface defects and pores. The wear mechanism gradually transforms from delamination wear to oxidative wear, and further evolves into abrasive wear and finally adhesive wear when the content exceeds 0.50 wt%.
    【Conclusion】 An appropriate addition of 0.25 wt% alumina whiskers significantly improves the hardness, friction coefficient and wear resistance of copper‑based friction materials by pore filling and load transfer strengthening. Excessive alumina whiskers lead to serious agglomeration, poor interface bonding and increased defects, which degrade mechanical and tribological properties. The wear mechanism is highly dependent on alumina whisker content. This study confirms that moderate alumina whisker reinforcement is an effective strategy to enhance the comprehensive performance of copper‑based friction materials for braking applications.
  • ZHANG Wangcheng, PENG Shichao, WANG Yilin, LIU Xu
    Powder Metallurgy Industry. 2026, 36(03): 107-113. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250069
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    【Objective】 The development of the wind power industry has placed higher demands on the wear resistance and stability of the friction coefficient of friction materials under low-speed and high-load conditions. In this paper, Al2O3, which has high hardness, good thermal conductivity and low cost, is used as the friction component to study the effect of its content on the performance of friction materials.
    【Method】 In this study, friction materials with Cu-Fe-Ni-graphite composition and Al2O3 content of 1%, 2% and 3% respectively were prepared by powder metallurgy process under a forming pressure of 400 MPa and a hot-pressing sintering process at 990 ℃ for 3 hours. The microstructure and composition uniformity of the friction materials were observed and analyzed by scanning electron microscopy. The mechanical properties of the friction materials were tested by an electronic universal testing machine and a Brinell hardness tester. The friction and wear properties of the friction materials were characterized by a friction material testing machine.
    【Result】 SEM and EDS analysis of the friction material indicated that the components are uniformly distributed in the matrix, which effectively enhances the friction and wear performance of the material. Tests reveal that when the mass fraction of Al2O3 in the friction material is 1% and 2%, the hardness and strength of the material are similar. However, when the mass fraction of Al2O3 increases to 3%, the hardness of the material increases while the density and strength decrease significantly. The friction material with a 2% mass fraction of Al2O3 has the best comprehensive mechanical properties, with a hardness of 32.67 HBW, a shear strength of 33.74 MPa, and a bonding strength of 29.70 MPa. The friction and wear tests show that the wear mechanism of the friction material is abrasive wear. As the content of Al2O3 increases, the wear of the friction material increases. The friction material with a 2% mass fraction of Al2O3 is more readily to achieve a stable coefficient of friction and has the highest coefficient of friction of 0.58 and a wear of 0.88 g.
    【Conclusion】 When the loss Al2O3 increases to an excessive content, it will reduce the density and strength of the friction material. The wear mechanism of the friction material is abrasive wear. With the increase of Al2O3 content, the number of friction cycles required before the friction coefficient stabilizes is reduced, and the friction coefficient first increases and then decreases, resulting in increased wear. When the mass fraction of Al2O3 in the friction material is 2%, the material has the best comprehensive performance.
  • WU Kaixia, ZHA Wusheng, WAN Haiyi, ZHAO Jiancheng
    Powder Metallurgy Industry. 2026, 36(03): 114-120. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250110
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    【Objective】 The objective of this paper is to prepare oxide dispersion strengthened (ODS) HT9 steel by vacuum hot pressing sintering, and to investigate the effects of different sintering temperatures and pressures on the mechanical properties, microstructure, phase composition and fracture morphology of the prepared ODS-HT9 steel.
    【Method】 ODS-HT9 steel was fabricated via vacuum hot pressing sintering. The density, HV, tensile strength and elongation of sintered samples under different temperatures and pressures were tested. The effects of sintering parameters on microstructure, phase composition and fracture morphology of ODS-HT9 steel were analyzed by means of optical microscope, XRD and SEM.
    【Result】 The increase of sintering temperature is beneficial to the adhesion of powder particles and the densification of samples. When the sintering temperature is 1 050 ℃, the relative density of the sample is the best, comprehensive properties are better, and the typical ductile fracture occurs. The hardness, tensile strength and elongation are 647HV, 916.1 MPa and 10.7%, respectively. With the increase of sintering pressure, the hardness, tensile strength and elongation of the samples increase gradually, and the density of the samples increases significantly. When the sintering pressure is more than 30 MPa, the increasing trend of density, hardness, tensile strength and elongation of the samples becomes slower.
    【Conclusion】 Sintering temperature and pressure exert pronounced effects on the microstructure and mechanical properties of ODS-HT9 steel. Moderate elevation of sintering temperature and pressure facilitates powder bonding and material densification, which further enhances the mechanical performances of sintered specimens.
  • WU Renjun, HOU Bolin, LIU Jinghang, WANG Jing, ZHANG Fangyang
    Powder Metallurgy Industry. 2026, 36(03): 121-127. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240175
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    This study investigates the effects of spark plasma sintering (SPS) on the microstructure, mechanical properties, and electrochemical corrosion behavior of NiCoCr multi-principal element alloys (MPEAs), with the aim of providing guidance for the fabrication of high-performance MPEA components using SPS technology. NiCoCr alloy powders were prepared via gas atomization. Preliminary sintering trials were conducted under three conditions: 900 ℃ for 5 minutes at 30 MPa, 1 000 ℃ for 5 minutes at 30 MPa, and 1 000 ℃ for 0 minute at 40 MPa. Based on the microstructural evaluation of these samples, optimal sintering parameters were selected for the main experiments: 900 ℃ for 15 minutes at 30 MPa, 1 000 ℃ for 15 minutes at 30 MPa, and 1 100 ℃ for 15 minutes at 30 MPa. The sintered samples were then subjected to microstructural characterization, uniaxial tensile testing, and electrochemical corrosion testing. As the sintering temperature increased, the alloy's strength decreased significantly, with the yield strength dropping from 835 MPa to 359 MPa, while plasticity improved markedly, with elongation rising from 22.5% to 61.6%. Furthermore, the alloy's work hardening rate was notably enhanced. Meanwhile, this alloy presents enhanced corrosion resistance, the corrosion current density (Icorr) decreased from 644 nA/cm2 to 57 nA/cm2, corrosion potential (Ecorr) increased from -0.369 mV to -0.249 mV, presenting.The NiCoCr MPEAs produced through SPS exhibited excellent mechanical properties. The alloy sintered at 1 100 ℃ for 15 minutes at 30 MPa demonstrated a favorable balance between mechanical strength and corrosion resistance.
  • Review and Progress
  • LI Xin, LI Qi, XIE Jun, LI Jinguo, LIANG Jingjing, LIU Xinggang
    Powder Metallurgy Industry. 2026, 36(03): 128-138. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240207
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    【Objective】 With the rapid development of fields such as aerospace, medical, and new energy vehicles, there arose a growing demand for the efficient and cost-effective preparation of high-performance metal powders. Therefore, this paper aimed to summarize the developmental history of numerical simulation and atomization mechanisms, reviewed advancements in gas atomization equipment, and systematically examined the effects of process parameters to promote the further development of gas atomization technology.
    【Method】 A comprehensive review of recent research on gas atomization technology was conducted. The study evaluated the application of numerical simulation models, specifically examining the Volume of Fluid (VOF) model for primary atomization and the Discrete Phase Model (DPM) for secondary atomization, to elucidate the complex, high-speed fragmentation processes. Additionally, it investigated the structural designs of atomizers, focusing on the differences between free-fall and close-coupled atomizers, as well as nozzle configurations. Finally, the paper analyzed the influence of critical process parameters, including atomization gas pressure, gas temperature, melt superheat, melt stream diameter, and the gas-to-liquid mass ratio, on the final powder characteristics.
    【Result】 Numerical simulations prove highly effective in visualizing unobservable phenomena, demonstrating how high-speed gas transforms metal melt into fine droplets that subsequently undergo spheroidization and solidification. Research on atomizer structures indicates that optimizing elements like the gas injection angle, delivery tube length, and nozzle aspect ratio significantly influences gas velocity and prevents nozzle blockage, thereby improving fine powder yield. Furthermore, process parameter adjustments play a pivotal role, increasing gas pressure and temperature generally enhances gas kinetic energy, leading to a reduction in powder particle size. Properly adjusting the melt superheat helps decrease surface tension and viscosity, which alters the droplet fragmentation mode and improves powder sphericity while reducing the formation of satellite particles.
    【Conclusion】 The review concluded that optimizing atomizer structures and process parameters directly dictated powder quality. It also suggested that future research needed to transition from single-factor analyses to investigating the interactive effects of multiple parameters. Furthermore, future developments required the creation of continuous numerical models that seamlessly coupled primary and secondary atomization stages, as well as the utilization of big data and imaging technologies to validate simulation results.
  • YANG Yajie, BAO Rui, YI Jianhong, LIU Liang
    Powder Metallurgy Industry. 2026, 36(03): 139-148. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240125
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    【Objective】 Nickel powder is a fundamental raw material in powder metallurgy, its physical and chemical characteristics are inextricably linked to the chosen preparation process. Among various synthesis routes, spray pyrolysis has demonstrated significant advantages in producing high-quality nickel-based powders. This paper systematically reviews several primary preparation methods—including mechanical milling, chemical reduction, hydrogen reduction, electrolysis, carbonyl decomposition, chemical vapor deposition (CVD), hydrothermal/solvothermal methods, and thermal decomposition. The objective is to compare their respective processes and key parameters while providing a technical basis for the advancement of spray pyrolysis technology.
    【Method】 A comparative study was performed to evaluate the mechanisms, advantages, and limitations of conventional nickel powder synthesis techniques. The research specifically focuses on the operational parameters of the spray pyrolysis method. It investigates the influence of diverse factors, such as atomization methods, precursor types, carrier gas compositions, additives, and reducing agents, on the final morphology and structural integrity of the nickel powder.
    【Result】 The findings indicate that while traditional methods like electrolysis or mechanical milling offer specific economic benefits, spray pyrolysis is superior for generating ultra-fine, spherical powders with high compositional homogeneity. The choice of atomization method significantly dictates the initial droplet size and subsequent particle fineness. Furthermore, the chemical nature of the precursors influences the kinetics of thermal decomposition, while the precise balance of carrier gases and reducing agents determines the oxidation state and surface morphology. The strategic application of additives was also found to effectively mitigate particle agglomeration, thereby enhancing powder dispersibility.
    【Conclusion】 The selection of a nickel powder preparation technique must balance performance requirements with production costs. Spray pyrolysis is a critical development direction for high-performance nickel-based materials due to its high controllability and process continuity. By fine-tuning the interplay of process parameters, customized microstructures can be achieved to meet specialized industrial needs. This review serves as a comprehensive reference for optimizing spray pyrolysis, facilitating technological upgrades in the industrial production of nickel-based powders.
  • PAN Bin, HAN Lei, QIAO Yongfei, TANG Fangfang
    Powder Metallurgy Industry. 2026, 36(03): 149-157. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250220
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    【Objective】 Additive manufacturing offered high design freedom and rapid fabrication capabilities for complex and precise components, and was widely applied in aerospace, biomedical, and automotive industries. However, the high cost and substantial consumption of metal powder severely hindered the large-scale industrial adoption of this technology. Recycling and reusing metal powder served as an effective approach to reduce production costs and achieve green sustainable manufacturing. This paper summarized the progress of domestic standardization of additive manufacturing metal powders, systematically reviewed the evolution of powder properties during recycling, and analyzed the influence mechanism of powder degradation on the mechanical performance of formed parts.
    【Method】 Taking commonly used additive manufacturing metal powders as the research objects, this paper summarized the evolution of key powder characteristics after multiple recycling cycles. The effects of powder recycling degradation on the mechanical properties and service stability of formed components were concluded. Based on recent experimental and theoretical investigations, three core technical strategies for metal powder recycling were summarized, and the advantages and existing limitations were compared.
    【Result】 Affected by the coupling effects of high-energy beam thermal shock, molten pool spattering, high-temperature consolidation, and forming chamber atmosphere, recycled metal powder exhibits an increased average particle size and a broader particle size distribution, accompanied by a continuous rise in oxygen content. Meanwhile, powder sphericity decreases along with increased surface roughness, and the proportion of irregular and flattened particles rises significantly. Mechanical test results show that aluminum alloy components are most adversely affected by powder recycling degradation. In contrast, reasonable recycling of titanium alloy, steel, and nickel-based superalloy powders can, to some extent, optimize or even improve certain mechanical properties of the formed parts.
    【Conclusion】 Powder recycling is an effective and feasible way to reduce the cost of powder bed fusion additive manufacturing and promote its industrialization. Powder recycling must balance raw material cost control against the service performance stability of formed components. Future research should focus on developing new additive manufacturing alloys with high oxidation resistance and low spattering tendency. Based on the interaction mechanism between the high-energy beam and powder, equipment and processes should be optimized to reduce powder spattering loss and extend powder recycling life, thereby supporting the large-scale, green, and high-quality sustainable development of metal additive manufacturing technology.
  • CHEN Zaisheng, WANG Yanxia
    Powder Metallurgy Industry. 2026, 36(03): 158-168. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250095
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    【Objective】 Soft magnetic composites (SMCs) have been widely used in power electronics, motor systems, and high-frequency electromagnetic devices because of their high electrical resistivity, low eddy-current loss, and flexible three-dimensional formability. With the rapid development of new energy equipment and high-frequency electronic systems, higher requirements have been placed on the magnetic performance, thermal stability, dimensional accuracy, and service reliability of SMCs. However, the preparation of high-performance SMCs still faces challenges such as unstable insulation coatings, insufficient densification, difficulty in fabricating complex structures, and limited microstructure control during heat treatment. This review aims to summarize recent progress in SMC preparation technologies and to clarify the influence of major processing routes on microstructure and magnetic properties.
    【Method】 This paper reviews the preparation technologies of SMCs from four aspects: insulation coating, forming, sintering, and heat treatment. Physical coating, sol-gel coating, and in situ growth are compared, together with the characteristics of organic, inorganic, and hybrid insulating materials. The effects of cold compaction, warm compaction, and hot pressing on densification and interface bonding are discussed. Conventional sintering and rapid sintering methods, such as spark plasma sintering and microwave sintering, are also analyzed. In addition, the roles of conventional annealing and magnetic-field-assisted heat treatment in stress relief and magnetic-domain regulation are summarized.
    【Result】 Existing studies show that insulation coating is a key approach for suppressing eddy-current loss and improving high-frequency performance, but coating type, thickness, and interface adhesion must be carefully controlled to avoid reducing permeability and magnetic flux density. Organic coatings have good processability but poor thermal resistance, whereas inorganic coatings offer better thermal stability but are prone to cracking and interfacial debonding. Hybrid coatings show greater potential, although their interfacial synergy requires further investigation. Improved densification through forming and sintering generally enhances magnetic response and mechanical strength, but excessive pressure or thermal exposure may damage the insulation layer and increase magnetic loss. Heat treatment, especially magnetic-field-assisted annealing, is effective in relieving residual stress, optimizing domain structure, reducing coercivity, and improving the high-frequency magnetic performance of SMCs.
    【Conclusion】 Future studies should focus on integrated optimization throughout the full preparation process, including the development of stable insulation systems with strong interfacial bonding, precision forming methods for complex components, efficient sintering routes that preserve insulation integrity, and refined heat-treatment strategies for stress relaxation and microstructure control. More attention should also be paid to the coupling relationship among coating structure, densification, thermal history, and magnetic loss, so as to support the large-scale fabrication and application of high-performance SMCs in high-frequency and high-efficiency devices.
  • Innovation and Communication
  • SHI Xiaorong, QIAN Xiachen, ZHANG Yanwei, ZHOU Tao, LIU Dongcang, WANG Chunyan
    Powder Metallurgy Industry. 2026, 36(03): 169-175. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240210
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    Powder Metallurgy is one of the main technologies for the production of gearbox interlock block. The interlock block has the characteristics of low stiffness, open slot and thin wall(3.5 mm). Parts are prone to deformation in the powder metallurgy production process, resulting in instability of the final product size. Through research and verification, this paper find out the main causes of deformation in the production process, and the process is optimized through the following 3 aspects. The forming die completed the “opening” to make the part “whole” to avoid the deformation caused by uneven thermal stress during sintering. At the same time the die adopt the form of “powder escape slot” to adjust the density of each step to ensure the overall density. The sandblasting was replaced with polishing, which reduced the influence of the uneven stress caused by sandblasting and led to the instability of machining size, and determined the optimal polishing time of 5 min. When machining slotting, rough machining reserved 0.3 mm wall thickness for finish machining, which solved the problem of deformation caused by clamping. Through the above improvement, the open slot size CPK is increased from 0.8 to 2.5, meeting the production requirement of CPK>1.33.