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10 December 2025, Volume 35 Issue 06
    

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    Experts Forum
  • CAO Yang, ZHAO Ruiwen
    Powder Metallurgy Industry. 2025, 35(06): 1-10. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250183
    Abstract ( ) Download PDF ( )   Knowledge map   Save
    This article provides a brief overview of the overall development and the breakdown of PM (powder metallurgy) products usage of China's powder metallurgy products industry. It covers the growth and market structure of the traditional powder metallurgy parts sector in China, as well as recent developments in automotive components, home appliance parts, and oil-impregnated bearings. The main technological advancements in China's powder metallurgy parts are briefly outlined. It also touches upon the impacts of the rapid development of new energy vehicles in China on the traditional ICE vehicle market and its subsequent effects on the traditional powder metallurgy parts industry. Additionally, it offers a brief analysis of the opportunities and challenges that the China's powder metallurgy products industry is likely to encounter in the future amid the rapid growth of emerging industries.
  • Research and Development
  • ZHANG Wei, GONG Xu, HAI Bozhan, WU Weichang, LIN Chenkang, LIU Kun
    Powder Metallurgy Industry. 2025, 35(06): 11-19. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240130
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    In order to elucidate the mechanical topological characteristics of iron powder pressing process, a numerical analysis model of iron powder pressing particles was established based on the discrete element theory, and the reliability of the model was verified by the pure iron powder pressing experiment conducted on a universal testing machine combined with the compression equation. By studying and simulating different friction factor conditions, combined with the definition of complex networks, and changing the topology-related parameters such as clustering coefficient, average degree and structural path length, the topological characteristics in the powder pressing process were explored. The results show that the number of L3 and L4 cycles composed of three and four particles increases gradually, while the number of L5, L6 and L6+ cycles composed of multiple particles decreases, indicating that the stability of the particle system is improved. In addition, the contact gap of powder particles decreases, the average degree and clustering coefficient of the system tend to decrease, and the structural path gradually becomes shorter, and the system gradually tends to densify. With the decrease of friction factor, the average degree and clustering coefficient increase, the structural path becomes shorter, and the compactness of the system is also improved, but at the same time, the fluidity becomes poor. This study reveals the evolution of the mesostructure of iron granular materials, expands the theoretical basis of the study of fine mechanics and topology of powder compression, and has guiding significance for the improvement of the dense forming of iron powder and different pressing processes.
  • HUA Qi, MO Wenjian, WANG Andong, LU Weihong, CHEN Pengfei, WANG Zhiyuan
    Powder Metallurgy Industry. 2025, 35(06): 20-27. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240091
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    With the increasing demand for lightweight phase change heat sink components for high power devices, Al-based wicks demonstrate high potential for application due to their low density. Permeability and capillary force, as the key properties of porous wicks, directly influence the heat transfer performance of heat sink components. However, due to the limitation of testing methods, the effect of powder properties on permeability and capillary force has rarely been reported. In this paper, Al-based porous wicks are prepared by a loosely packed sintering process, using Al powders of different sizes and morphologies with suitable flux. The differences between pore characteristics, permeability and capillary properties, and flexural strength of the porous wicks are compared in detail, which reveal their relationship with Al powder size and morphology. The results show that powder size and morphology have a significant effect on the pore characteristics of wicks. Using the irregularly shaped 180-106 μm Al powder, the porous wick can maintain high porosity while possessing high strength, which exhibits the best overall performance, with a porosity of 40.84%, a permeability of 2.94×10-11 m2, a capillary force of 0.92 kPa, and a flexural strength of 26.05 MPa.
  • ZHANG Mingjun, LIU Zhongjun, JING Yuan, WANG Yanying, LI Qi, MENG Xiantao
    Powder Metallurgy Industry. 2025, 35(06): 28-36. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240135
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    A composite gradient porous membrane material was successfully prepared using a combination of cold isostatic pressing, centrifugal deposition molding technology, and vacuum sintering, with 316L porous stainless steel as the matrix and ZrO2 as the membrane layer. The phase composition, microporous structure morphology, and pore properties of porous materials were analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), and a porous material integrity tester. The influence of sintering temperature on the pore structure morphology, air permeability coefficient, and pore size distribution of 316L-ZrO2 composite gradient porous membrane material was studied, and finally its filtration application in the treatment of oily and saline wastewater was studied using dead-end filtration technique. The results show that by introducing a correction factor K into the formula for calculating the thickness of the gradient membrane layer, accurate control of the membrane thickness can be achieved. In this experiment the K value ranged from 0.21 to 0.25. The permeability of the membrane material decreases gradually as the sintering temperature rises, and the reduction in the permeability coefficient is more pronounced at 700-800°C. Meanwhile, the average pore size of the membrane layer becomes smaller, decreasing from 0.28 µm to 0.18 µm. The 316L-ZrO2 composite gradient porous membrane can effectively remove suspended solids from oily and saline wastewater, but has poor removal effects on COD, ammonia nitrogen, and soluble salts.
  • CHEN Xi, TAN Jianjun, HU Peng, DENG Bo, GONG Jiacheng, HUANG Boxiang
    Powder Metallurgy Industry. 2025, 35(06): 37-40. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240115
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    The electrode induction melting gas atomization (EIGA) technology was successfully used to overcome the technical difficulties in preparing spherical rare earth gadolinium powder. The effect of different atomization pressures on the particle size of the powder was studied. The optimal rare earth gadolinium atomization process for this experiment is: atomization power of 43 kW, rod descent speed of 20 mm/min, rotation speed of 5 r/min, and atomization pressure of 5.0 MPa. The apparent morphology, particle size, and flowability of the spherical powder were measured using scanning electron microscopy, particle size analyzer, and Hall flowmeter. After 60 mesh sieving, the performance of gadolinium powder is determined as follows: powder particle size D10=22.29 μm, D50=59.71 μm、D90=121.3 μm, liquidity of 28.33 s/50g, loose density of 4.36 g/cm3, compacted density of 5.15 g/cm3, good sphericity, and no introduction of non-metallic inclusions.
  • LIU Jiying, LIU Fei
    Powder Metallurgy Industry. 2025, 35(06): 41-45. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240100
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    in this paper, ultrafine silver powder was prepared by liquid-phase chemical method. The effects of feeding rate, reaction temperature, concentration of silver nitrate, refining dose and alkali temperature on the properties of ultrafine silver powder were studied, the morphology was observed by scanning electron microscopy (SEM). The results show that when the AgNO3 concentration, AgNO3 feeding rate, reaction temperature, refining dose and alkali temperature are 0.15 mol/L、200 L/S、55 ℃、35 g、30 ℃, the agglomerations of ultrafine silver powder are less, the particle sizes are uniform and the distribution is concentrated, show excellent performance.
  • QIN Yuanyuan, LI Zhongxiang
    Powder Metallurgy Industry. 2025, 35(06): 46-50. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240157
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    The influence of physical properties of tantalum powder on the shapeability of tantalum anode blocks was analyzed. The results show that the pressing and shaping of tantalum electrolytic anode blocks is closely related to the physical properties of tantalum powder, such as fluidity, particle size distribution, and the size of the aggregated particles after subsequent agglomeration treatment. When the Fisher particle size of the sample increases from 6 μm to 16.4 μm and the particle size distribution span decreases from 1.76 to 0.96, the flowability improves significantly. Concurrently, the compactibility of the tantalum powder is markedly enhanced, with compressive strength increasing from 4.6 MPa to 14.6 MPa, and the bonding with tantalum wire leads become more robust.
  • YUAN Dapeng, YANG Wen'an, NAN Jian, HU Jiaqi, XIE Liangjun, LIU Qingwei
    Powder Metallurgy Industry. 2025, 35(06): 51-56. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240156
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    Iron-based amorphous coatings were fabricated by high-velocity oxy-fuel (HVOF) spraying. The effects of oxygen flow rate and powder feed rate on the average thickness per layer, porosity, and Vickers hardness of the coatings were systematically investigated. The average thickness per layer was mainly affected by the combustion degree between aviation kerosene and oxygen, as well as by the powder feeding rate. When the oxygen flow was 0.849 6 or 0.873 2 m3/min, i.e., close to the complete combustion ratio between oxygen and kerosene, the coating exhibites the highest average thickness per layer. With further increase in oxygen flow, the average thickness decreases, whereas it increases gradually with increasing powder feeding rate. The porosity of the coatings is jointly affected by the surface oxidation of powder particles and by their temperature and velocity, which are influenced by the heating and acceleration effects of the combustion gas during spraying. No clear mathematical relationship is found between porosity and powder feeding rate. As oxygen flow increases, porosity first increases and then decreases, reaching a peak at 0.896 8 m3/min. The micro-Vickers hardness of the coatings is mainly determined by the thermal input to the powder particles from the high-temperature, high-velocity gas flow. Higher thermal input led to lower hardness. Increasing the powder feeding rate also reduces the hardness. With increasing oxygen flow, the microhardness first decreases and then increases, eventually reaching the lowest value at 0.873 2 m3/min. Given the result of porosity examination, the optimal process parameters are determined as an oxygen flow of 0.849 6 m3/min and a powder feeding rate of 3.8 g/min, under which the coating exhibites the lowest porosity (1.8%), an average single-layer thickness of 21.4 μm, and a Vickers hardness of 810.8 HV.
  • MENG Kui, FAN Chenyang, WANG Chengsong, SONG Tao, WANG Pei, HAN Tian
    Powder Metallurgy Industry. 2025, 35(06): 57-64. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240138
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    Multi-metal laser additive manufacturing is an emerging technology for manufacturing complex parts with excellent overall performance. In this study, mutant functional gradient materials with 100% compositional change of Ti65/Q355D were prepared by laser direct energy deposition. Microstructure analysis, energy spectrum analysis, transmission electron microscopy analysis, microhardness and friction property tests were used to characterize and analyze the microstructure evolution, compositional segregation, microcrack formation and mechanical properties of the materials. The results show that the microstructures of Ti65 and Q355D are dominated by columnar dendrites and equiaxed dendrites, respectively. The compositional segregation of Ti65 on the Q355D side is induced by Marangoni convection effect, and the compositional segregation of the two metals and the different physical properties of the two metals are the main reasons for the inclined cracking near the interface. The two metals diffused each other at high temperatures, and the microhardness increases nearly linearly from Q355D (163HV) to Ti65 (529 HV). The wear surface of Q355D is caused by the combination of abrasive, adhesive wear and micro-cutting, resulting in grooves, chips, spalling and micro-cracks. The wear surface of Ti65 containes fine debris and smooth shallow grooves, resulting in abrasive wear and slight adhesive wear. Deposition of Ti65 on the surface of Q355D can significantly improve the microhardness and friction and wear properties of the specimens, providing data support for the practical application of gradient materials.
  • WANG Zimin, LIAO Jianwen, DENG Zhigang
    Powder Metallurgy Industry. 2025, 35(06): 65-69. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240050
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    High voltage rare earth permanent ferrite Ca0.85-yLaySr0.15Fe2n-0.3Co0.3O19-δ was prepared by ceramic technology. The magnetic characteristics, voltage resistance and microstructure of the products were detected and analyzed by pressure tester, permanent ferrite measuring instrument and scanning electron microscope. The results show that under specific technological conditions, the magnetic properties and voltage resistance of the material are significantly improved with the replacement of n and La in the main formula and the addition of appropriate SiO2. When n=5.3, y=0.36, and the pre-sintering temperature is at 1 260 ℃, the pre-sintering material come into being. Then during fine grinding, 0.15%SiO2 is added. Combined with the slow heating (1 ℃/min) and fast cooling sintering (10 ℃/min) process of the formed compact between 1 100-1 180 ℃, rare earth permanent magnet ferrite with (BH)max to 36.37 kJ/m3 excellent magnetic properties and high pressure resistance (AC1 500 V, 2.4 mA leakage current) can be obtained.
  • ZHANG Liang, WAN Hao, CHEN Yue, LIU Guanglei
    Powder Metallurgy Industry. 2025, 35(06): 70-80. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240182
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    In order to further improve the accuracy of compositional control of Fe-Mn-Si system memory alloys to ensure their properties, the interaction of three main process parameters, namely, ball milling time, sintering temperature, and sintering time, on the densities, microhardnesses, tensile strengths, and shape regaining rates of Fe-based memory alloys was investigated by means of powder sintering, with the aid of the response surface method. The results show that ball milling time, sintering temperature, and sintering time all have an important effect on alloy properties. Through the design of response surface method experiments and results analysis, a set of more accurate mathematical models could be obtained to reflect the magnitude of the influence of process parameters on the properties of the alloy and the role of the law, but also to establish the corresponding relationship between process parameters and properties. It is verified that the error between the model predicted values and the real experimental values of each performance index is 4.67% at the maximum and 0.77% at the minimum for the specimens prepared with the two sets of optimal process parameters within and outside the experimental ranges recommended by the resulting model, and the alloy compositions are controlled more accurately. The sintering and forming process of Fe-based memory alloy powder based on response surface method is instructive for engineering applications.
  • LIU Yiran, LI Lei, LI Yunjin, PEI Haoyu
    Powder Metallurgy Industry. 2025, 35(06): 81-86. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240140
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    The effects of annealing temperature on the microstructure, mechanical properties and tribological and wear properties of Al-Mg alloy with Er (0.14%) and Zr (0.2%) were studied by means of optical microscope, scanning electron microscope, friction and wear testing machine and tensile testing machine. The results show that with the increase of annealing temperature, the grain boundary precipitates distribute evenly, the second phase of Al3 (Er,Zr) particles gradually increase in size, the surface columnar elongated crystals gradually fuse, and the microstructure becomes uniform. The average diameter and depth of fracture dimples gradually increase and deepen. The tensile strength and microhardness of the alloy decrease gradually, while the elongation increases gradually, and the plastic deformation ability increases significantly.
  • LIU Jun, HUO Junmei, LIU Jinxu, LIU Wei, LI Zhekun, YU Hai
    Powder Metallurgy Industry. 2025, 35(06): 87-94. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250147
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    In this paper, the effects of laser selective melting process parameters on the forming defects, microstructure and high temperature stress rupture properties of GH3625 alloy were studied. The results show that in the process of selective laser melting, when the bulk energy density is too low, a small number of unmelted defects and more holes are observed in the metal phase. With the increase of bulk energy density, there are only a few voids in the metal phase, no incomplete fusion defects. After solution treatment, the microstructure of samples with different bulk energy density shows the morphology of transverse equiaxed crystal and longitudinal columnar crystal. The high temperature rupture life and elongation after fracture of longitudinal specimens are higher than those of transverse specimens. When there are only tiny holes in the sample, the transverse and longitudinal rupture life are more than 70 h, and the longitudinal elongation after fracture is more than 23%. The rupture fracture shows that the cracks originate from the surface of the sample. The main fracture mode of the transverse sample is that the grain boundary microcracks propagate and connect to form the main crack, and the main fracture mode of the longitudinal sample is that the grain boundary diffusion type holes gather microcracks and connect to form the main crack. The results show that the high temperature rupture life is significantly reduced when there are strip-shaped non fusion defects in the specimen, the rupture life of the transverse and longitudinal specimens is as low as 19 h and 28.7 h, respectively, and the longitudinal elongation after fracture is reduced to 9%, which is mainly because the strip-shaped non fusion defects as micro cracks accelerate the connection and propagation of the rupture crack.
  • XIAO Yubin, LI Lin, TIAN Kai, LEI Jin, LIU Zicong, YUAN Jianping
    Powder Metallurgy Industry. 2025, 35(06): 95-100. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240097
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    In this paper, by changing the time of aging treatment, comparative study of aging treatment on the organization and tensile properties of selective laser melting (SLM) forming AlMgScZr alloy, analysis of the organization morphology and tensile properties of the trend of change, for the SLM AlMgScZr heat treatment process to provide data reference and theoretical support. The results show that after aging treatment for 2, 4 and 6 h, the tensile strength of the alloy reaches 507.9, 538.5 and 575.4 MPa, which are increased by 35%, 43% and 52%, respectively, compared with that of the alloy without aging treatment, this is due to the fact that the alloy precipitates a large number of precipitated phases with the increase of aging treatment time, and the increase of Al3(Sc,Zr) content, which hinders the dislocation movement and produces precipitation strengthening and fine grain strengthening. A large number of tough nests are present in the fracture morphology of the alloy, and the content of cleavage surfaces increases with aging treatment time.
  • LI Ming, SHANG Chuanbao, LIU Shun, ZHANG Huijuan, SUN Xiaofeng, SHANG Yutao
    Powder Metallurgy Industry. 2025, 35(06): 101-106. https://doi.org/10.13228/j.boyuan.issn1006-6543.20230164
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    Focusing on the sensitivity of WNiFe alloys to tensile rate, 93WNiFe alloy was selected as the research object. Through uniaxial static tensile tests under different tensile rates, combined with fracture morphology analysis, the effects of tensile rate on its tensile properties (tensile strength, elongation after fracture) and fracture mechanism were investigated, and the sensitivity coefficient was introduced to quantify the sensitivity. The results show that 93WNiFe alloy has high sensitivity to tensile rate, presenting the characteristic of "high sensitivity in low rate range and low sensitivity in high rate range". As the tensile rate increases from 0.18 mm/min to 19.29 mm/min, the tensile strength increases from 889 MPa to 940 MPa (with an increase of 5.7%), and the elongation after fracture decreases from 32.5% to 22.0% (with a decrease of 32.3%). The sensitivity coefficient indicates that the sensitivity is the highest in the 0.18→0.45 mm/min range (tensile strength S≈48.15 MPa·min/mm, elongation after fracture S≈-11.11%·min/mm), while it decreases significantly in the 12.06→19.29 mm/min range (tensile strength S≈0.28 MPa·min/mm, elongation after fracture S=0). On the micro mechanism, the increase of tensile rate leads to the transformation of fracture mode from "dominated by tungsten-tungsten interface separation" to "dominated by transgranular fracture of tungsten particles", which is the main reason for the improvement of tensile strength. Meanwhile, the proportion of fracture phase decreases from 3.68% to 0.66%, resulting in the reduction of elongation after fracture. The research results can provide a theoretical reference for the application of 93WNiFe alloy under different service rate conditions.
  • WU Chao, LIU TONG, LIU Jianming, ZHANG Xin
    Powder Metallurgy Industry. 2025, 35(06): 107-114. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240146
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    The labyrinth seal is an important pneumatic sealing structure in aircraft engines. In order to prevent wear and damage between the labyrinth and the metal honeycomb during operation, a nickel aluminum alumina wear-resistant protective coating was prepared on the surface of the labyrinth by plasma spraying. The coating is complete and well bonded. The service performance of the coating under simulated working conditions was tested using a high-temperature and high-speed abrasion tester. The results show that after scraping with labyrinth and honeycomb, significant plastic deformation occurres in the honeycomb. The labyrinth mainly undergo cutting and wear, with obvious application, adhesion, and accumulation of honeycomb material on the surface. Increasing the line speed and feed depth can aggravate the damage and deformation of the honeycomb and the adhesion to the surface of the grate teeth. The tip of the labyrinth do not show significant wear and deformation, indicating that the coating do not undergo large peeling during the grinding and scraping process, but is cyclically worn by honeycomb layers, and the coating provides good protection for the labyrinth. Under the testing conditions of a linear velocity of 300 m/s and a feed depth of 300 μm, the maximum values of tangential and radial forces during impact grinding are 999.51 N and 582.52 N, respectively, achieving a small gap structure for the rotor and effectively ensuring the sealing effect of the gas path.
  • WU Kaixia, ZHA Wusheng, FANG Xiumei, XIA Yiwen, GUO Lihong, HUANG Hui, HU Li
    Powder Metallurgy Industry. 2025, 35(06): 115-119. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240127
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    The titanium coatings were prepared by mechanical coating technology on the surface of ZrO2 balls with 1mm diameter,and then the titanium coatings were oxidized to titanium oxide coatings at 500 ℃ for 5 h. The cross-section morphology of titanium coatings were analyzed by metallographic microscope, and then the influence of different milling speed and milling time on the formation of coatings were studied. The phase composition of titanium oxide coatings were analyzed by X-ray diffractometer (XRD), and the photocatalytic properties of different coating thicknesses and different coating dosages were measured. The results show that the increase of ball mill speed will increase the energy input of ball mill system per unit time, thus increasing the deposition rate of powder material and thickening the coatings. In a certain range of milling time, the coating thickness increases with the increase of milling time, and the photocatalytic performance of the coating increases with the increase of the coating thickness, and finally tended to be stable. The increase of catalyst dosage will increase the degradation rate of solution, but too much catalyst dosage will decrease the degradation rate of solution. The best photocatalytic performance of the coatings is 88.4% when the milling time is 30 h and the dosage is 1 g/mL. And the coatings have a good reusability.
  • Review and Progress
  • ZHANG Jia, ZHANG Junhao, JIA Qinggong, JIAO Hua
    Powder Metallurgy Industry. 2025, 35(06): 120-129. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240141
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    This paper systematically reviews the research progress and applications of light-curing 3D printing technology in various fields. Firstly, the principles and main methods of light-curing technology are introduced, including stereolithography (SLA), mask projection stereolithography (MPSL), two-photon polymerization (TPP), and digital light processing (DLP), with analysis of their technical characteristics. Secondly, the composition, modification methods, and research status of photosensitive resins for performance enhancement are discussed in detail. The focus is on the applications of light-curing technology in medical fields (such as dental restoration, tissue engineering scaffolds, tumor models, and flexible monitoring sensors), as well as in electronic information and mechanical manufacturing. Finally, the future development directions of light-curing technology are prospected, emphasizing the key role of material innovation and process optimization in promoting the integration of medicine and engineering and intelligent manufacturing.
  • SU Fengge, ZHENG Zhuo, HE Shanhai
    Powder Metallurgy Industry. 2025, 35(06): 130-141. https://doi.org/10.13228/j.boyuan.issn1006-6543.20250031
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    Sinter hardening typically refers to the process during the later stages of continuous sintering where the material partially or fully transforms into martensite at relatively low cooling rates (1-3 °C/s). Compared to traditional heat treatment processes, material strengthening can be achieved simply by controlling the cooling rate in the later stages of sintering, offering a cost advantage in the process. This method is also known as the one step process. This article analyzes the research work of domestic and foreign scholars on sintered hardening powder in recent years, and elaborates on the research progress of sintered hardening powder from the aspects of composition design, alloy elements, and the influence of sintering processes on hardening properties. It also summarizes some of the technical issues currently encountered with sinter hardening powders, expanding the selection of alloy elements and improving the sintering hardening process in a targeted manner will be the development direction of sintering hardening powder in the future. Expanding the selection of alloy elements and improving the sintering hardening process in a targeted manner will be the development direction of sintering hardening powder in the future.
  • YE Xuan, CHEN Yanfang, QIN Ling
    Powder Metallurgy Industry. 2025, 35(06): 142-155. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240059
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    Fe-based powder metallurgy oil-bearing materials trend to can't simultaneously have both high mechanical properties and good self-lubricating properties, which seriously hinders the development and application of Fe-based oil-bearing. Reinforcement phase, lubrication phase, preparation process and pore structure are depicted to briefly describe Fe-based powder metallurgy oil-bearing materials. It is shown that the development of a kind of Fe-based powder metallurgy oil-bearing materials with good lubrication and high mechanical properties is one of the future development trends of Fe based composite materials.
  • Innovation and Communication
  • LI Hong, ZHANG Xiaodan, ZHANG Chao, XING Xintao, YAN Zhenhua, ZHANG Shulan
    Powder Metallurgy Industry. 2025, 35(06): 156-164. https://doi.org/10.13228/j.boyuan.issn1006-6543.20240060
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    Temperature range of solid-liquid phase line of self-fluxing alloy powder is an important considering factor for the setting of welding process parameters, and it is also an important parameter affecting the properties of such materials and thermal spraying、 laser cladding and 3D printing quality. It is particularly important to determine the precise solid-liquidus temperature range of self-fluxing alloy powder. In this paper, the melting and solidification curves of self-fluxing alloy powder were measured by DSC according to the standard YS/T533-2006, and the correct method of determination of solid-liquidus and the optimal measurement parameter were discussed. The experimental results show that, the obtained onset solidification temperature is lower than the onset melting temperature during the heating process because of the existence of supercooling during solidification, which is inconsistent with the characteristic that the liquidus is higher than the solid phase line in the binary phase diagram. The solid-liquidus of the self-fluxing alloy should be measured according to the melting curve, and the melting starting and ending temperatures correspond to the solid-phase and liquidus temperatures, respectively. In addition, the experimental results of different heating rates and sample mass show that the test results have good repeatability when the heating rate is 4-10 ℃/min and the sample mass is 5-50 mg, 10 ℃ and 15 mg is recommended.