Characterization of pre-alloyed TiAl powder and its microstructure characteristics after hot-pressing
KANG Fu-wei1,WANG Shan-shan1,SUN Jian-fei2,LIU Na3
(1. School of Materials Science and Engineering, Harbin University of Science and Technology, Harbin 150040, China 2. School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China 3. Science and Technology on Advanced High Temperature Structural Materials Laboratory, Beijing Institute of Aeronautical Materials, Beijing 100095, China)
Abstract:The TiAl-based pre-alloy powder prepared by gas atomization process and its vacuum hot pressing microstructure were studied by laser particle size analyzer, metallographic microscope and scanning electron microscope (SEM). The results show that the pre-alloyed powder particles prepared by gas atomization process are fine and have good sphericity. The particle size is mainly distributed in the range of 20.0-40.0 μm. The powder particles with different size have different surface and internal morphology. The interior and surface of the small size powder show no histological features. With the further increase of the powder particle size, the surface and internal structure of the powder gradually change from the cellular dendrite to the dendrites. After vacuum hot-pressing, the dense and uniform microstructure is obtained and the internal microstructure is duplex.
康福伟,王珊珊,孙剑飞,刘 娜. TiAl预合金粉末表征及后续热压烧结组织特点[J]. , 2018, 28(01): 38-44.
KANG Fu-wei,WANG Shan-shan,SUN Jian-fei,LIU Na. Characterization of pre-alloyed TiAl powder and its microstructure characteristics after hot-pressing. , 2018, 28(01): 38-44.
[1]Wang J W, Wang Y, Liu Y, et al.Densification and microstructural evolution of a high niobium containing TiAl alloy consolidated by spark plasma sintering[J]., 2015, 64:70-77
[2]Clemens H, Smarsly W.Light-weight intermetallic titanium aluminides-status of research and development[J].Advanced Materials Research, 2011, 278:551-556
[3]陈玉勇, 杨非, 孔凡涛, 等.TiAl合金的热加工、组织和性能[J].中国材料讲展, 2010, (03):12-17
[4]杨锐.钛铝金属间化合物的进展与挑战[J].金属学报, 2015, (02):129-147
[5]Schwaighofer E, Clemens H, Mayer S, et al.Microstructural design and mechanical properties of a cast and heat-treated intermetallic mufti-phase γ-TiAl based alloy[J].Intermetallics, 2014, 44:128-140
[6]Wang Y, Liu Y, Yang G Y, et al.Hot deformation behaviors of β phase containing Ti-43Al-4Nb-1.4W-based alloy[J].Mater Sci Eng A, 2013, 577:210-217
[7]Voisin T, Muriel J P, Monchoux H, et al.Microstructures and mechanical properties of a multi-phase β-solidifying TiAl alloy densified by spark plasma sintering[J].Acta Materialia, 2014, 73:107-115
[8]陈玉勇, 张树志, 孔凡涛, 等.新型β-γ合金的研究进展[J].稀有金属, 2012, 36(1):154-160
[9]Schloffer M, Schmoelzer T, Mayer S, et al.The characterisation of a powder metallurgically manufactured TNM(TM) titanium aluminide alloy using complimentary quantitative methods[J].Practical Metallography, 2011, 48(11):594-604
[10]Vajpai S K, Ameyama K.A novel powder metallurgy processing approach to prepare fine-grained Ti-rich TiAl-based alloys from pre-alloyed powders[J].Intermetallics, 2013, 42:146-155
[11]刘咏, 黄伯云, 周科朝, 等.热等静压对粉末冶金TiAl合金显微组织和相成分的影响[J].粉末冶金技术, 2001, (03):165-169
[12]吴杰, 徐磊, 郭瑞朋, 等.粉末冶金----合金的制备及力学性能影响因素[J].材料研究学报, 2015, 29(2):127-134
[13]Luo J S, Voisin T, Monchoux J P, et al.Refinement of lamellar microstructures by boron incorporation in GE-TiAl alloys processed by spark plasma sintering[J].Intermetallics, 2013, 36 :12-20
[14]Huang Y J, Wang Y, Fan H B, et al.A TiAl based alloy with excellent mechanical performance prepared by gas atomization and spark plasma sintering[J].Intermetallics, 2012, 31:202-207
[15]王建军.中国雾化制粉技术现状简介[J].粉末冶金工业, 2016, 26(5):1-4
[16]曹勇家, 钟海林, 郝权, 等.粉末冶金生产上艺的两大发展[J].粉末冶金工业, 2011, 21(1):45-53
[17]王刚, 郑卓, 常立涛, 等.预合金粉末的表征和后续致密化显微组织特点[J].金属学报, 2011, 47(10):1263-1269
[18]杨冬野.钛铝合金气雾化及其烧结成形的组织与相结构[D]. 哈尔滨: 哈尔滨工业大学(博士学位论文), 2015.
[19]Zeoli N, Gu S.Computational simulation of metal droplet break-up,cooling and solidification during gas atomisation[J].Computational Materials Science, 2008, 43(2):268-278
[20]Shu S L, Qin F, Ring B, et al.Effect of strain rate on the compression behavior of TiAl and TiAl-2Mn alloys fabricated by combustion synthesis and hot press consolidation[J].Intermetallics, 2013, 43:24-28